Details
Chinese Factory Supply Wholesale 4-N-BUTOXYBENZOYL CHLORIDE 33863-86-4 with Cheap Price
- Molecular Formula: C11H13 Cl O2
- Molecular Weight: 212.676
- Vapor Pressure: 0.000649mmHg at 25°C
- Refractive Index: n20/D 1.5495(lit.)
- Boiling Point: 309.2°Cat760mmHg
- Flash Point: 115°C
- PSA： 26.30000
- Density: 1.123g/cm3
- LogP: 3.24450
4-N-BUTOXYBENZOYL CHLORIDE(Cas 33863-86-4) Usage
|
General Description |
4-N-Butoxybenzoyl chloride is a chemical compound with the molecular formula C11H13ClO2. It is a derivative of benzoic acid and belongs to the class of organic compounds known as benzoyl chlorides. 4-N-BUTOXYBENZOYL CHLORIDE is commonly used in the synthesis of pharmaceuticals, agrochemicals, and other specialty chemicals. It is an important intermediate in the production of various drugs and is also used in the manufacturing of dyes and pigments. 4-N-Butoxybenzoyl chloride is a colorless to pale yellow liquid with a pungent odor and is highly reactive, particularly with water and alcohols. It is important to handle and store this chemical with care due to its hazardous nature and potential to cause irritation to the skin, eyes, and respiratory system. |
InChI:InChI=1/C11H13ClO2/c1-2-3-8-14-10-6-4-9(5-7-10)11(12)13/h4-7H,2-3,8H2,1H3
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33863-86-4 Process route
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-
1498-96-0
4-butoxybenzoic acid
-
-
33863-86-4
4-(n-butyloxy)benzoyl chloride
| Conditions | Yield |
|---|---|
|
4-butoxybenzoic acid;
With
N,N-dimethyl-formamide;
In
dichloromethane;
at 0 ℃;
for 0.0833333h;
With
oxalyl dichloride;
In
dichloromethane;
at 20 ℃;
for 12h;
|
100%
|
|
With
thionyl chloride;
|
83%
|
|
With
thionyl chloride;
|
|
|
With
phosphorus pentachloride;
|
|
|
With
thionyl chloride;
In
benzene;
for 3h;
Heating;
|
|
|
With
thionyl chloride;
for 2h;
Heating;
|
|
|
With
thionyl chloride;
for 0.5h;
Heating;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
In
toluene;
at 60 - 70 ℃;
for 0.5h;
|
|
|
With
thionyl chloride;
for 2h;
Heating;
|
|
|
With
thionyl chloride;
for 0.5h;
Heating;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
Heating;
|
|
|
With
pyridine; thionyl chloride;
In
toluene;
Heating;
|
|
|
With
thionyl chloride;
Heating;
|
|
|
With
thionyl chloride;
In
benzene;
|
|
|
With
thionyl chloride;
In
benzene;
Heating;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
at 90 ℃;
for 4h;
|
|
|
In
thionyl chloride;
|
|
|
In
thionyl chloride;
|
|
|
With
thionyl chloride;
In
toluene;
at 20 ℃;
for 24h;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
Heating;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
thionyl chloride; triethylamine;
at 0 ℃;
Reflux;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
for 3h;
Reflux;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
tetrahydrofuran;
at 20 ℃;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
for 3h;
Reflux;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride;
for 3h;
Reflux;
|
|
|
With
thionyl chloride;
|
|
|
With
phosphorus pentachloride;
In
toluene;
for 4h;
Heating;
|
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.5h;
Reflux;
|
|
|
With
thionyl chloride;
Heating;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
thionyl chloride;
for 3h;
Reflux;
|
|
|
With
hydrogenchloride; thionyl chloride;
In
water;
|
|
|
With
oxalyl dichloride; N,N-dimethyl-formamide;
for 1h;
Inert atmosphere;
|
|
|
With
phosphorus pentachloride;
In
toluene;
|
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 3h;
Inert atmosphere;
|
|
|
With
thionyl chloride;
for 2h;
Reflux;
|
|
|
With
thionyl chloride;
for 3h;
Reflux;
|
|
|
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
|
|
|
With
thionyl chloride;
In
benzene;
at 80 ℃;
for 3h;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
thionyl chloride;
for 2h;
Reflux;
|
|
|
With
phosphorus pentachloride; trichlorophosphate; phosphorus trichloride;
In
1,4-dioxane; tetrachloromethane; chloroform;
at 45 ℃;
Darkness;
Large scale;
|
-
-
99-96-7
4-hydroxy-benzoic acid
-
-
33863-86-4
4-(n-butyloxy)benzoyl chloride
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
2
steps
1: KOH / ethanol
2: SOCl2
With
potassium hydroxide; thionyl chloride;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: KOH / ethanol / Heating
2: SOCl2
With
potassium hydroxide; thionyl chloride;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: aqueous KOH-solution
2: thionyl chloride
With
potassium hydroxide; thionyl chloride;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: methanol / Reflux
2: thionyl chloride
With
thionyl chloride;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / 3 h / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
With
thionyl chloride;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / ethanol / 25 h / Reflux
2: thionyl chloride / 3 h / Reflux
With
thionyl chloride; potassium hydroxide;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / ethanol
2: thionyl chloride / Heating
With
thionyl chloride; potassium hydroxide;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / ethanol / 8 h / Reflux
2: thionyl chloride / 3 h / Reflux
With
thionyl chloride; potassium hydroxide;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: methanol
2: thionyl chloride
With
thionyl chloride;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / ethanol
2: thionyl chloride
With
thionyl chloride; potassium hydroxide;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: methanol
2: thionyl chloride
With
thionyl chloride;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol
2: thionyl chloride; hydrogenchloride / water
With
hydrogenchloride; thionyl chloride; potassium hydroxide;
In
methanol; water;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / ethanol
2: thionyl chloride / Heating
With
thionyl chloride; potassium hydroxide;
In
ethanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / 3 h / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
|
|
|
Multi-step reaction
with
2
steps
1: potassium hydroxide / methanol / Reflux
2: thionyl chloride / 2 h / Reflux
With
thionyl chloride; potassium hydroxide;
In
methanol;
1: |Williamson Ether Synthesis;
|
33863-86-4 Upstream products
-
1498-96-0
4-butoxybenzoic acid
-
99-96-7
4-hydroxy-benzoic acid
-
120-47-8
Ethyl 4-hydroxybenzoate
-
5365-43-5
ethyl 4-butoxybenzoate
33863-86-4 Downstream products
-
67032-42-2
4-butoxy-benzoic acid-[β-(2-methyl-piperidino)-isopropyl ester]; hydrochloride
-
67032-47-7
4-butoxy-benzoic acid-[3-(4-methyl-piperidino)-propylester]; hydrochloride
-
63916-68-7
4-butoxy-benzoic acid-[3-(2-methyl-piperidino)-propyl ester]
-
110331-49-2
4-butoxy-benzoic acid-(1,1-dimethyl-3-piperidino-propyl ester)
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