Details
Buy Quality 7-METHOXY-3,4,5,6-TETRAHYDRO-2H-AZEPINE 2525-16-8 In Stock with Immediately Delivery
- Molecular Formula: C7H13NO
- Molecular Weight: 127.186
- Vapor Pressure: 3.95mmHg at 25°C
- Refractive Index: n20/D 1.463(lit.)
- Boiling Point: 155.2 °C at 760 mmHg
- PKA: 5.94±0.20(Predicted)
- Flash Point: 51.1 °C
- PSA： 21.59000
- Density: 1 g/cm3
- LogP: 1.04090
7-METHOXY-3,4,5,6-TETRAHYDRO-2H-AZEPINE(Cas 2525-16-8) Usage
|
Synthesis Reference(s) |
Organic Syntheses, Coll. Vol. 4, p. 588, 1963Tetrahedron Letters, 20, p. 4671, 1979 DOI: 10.1016/S0040-4039(01)86679-X |
InChI:InChI=1/C7H13NO/c1-9-7-5-3-2-4-6-8-7/h2-6H2,1H3
2525-16-8 Relevant articles
Synthesis and bronchodilatory activity of some nitrogen bridgehead compounds
Jindal, Dharam Paul,Bhatti, Ravinder Singh,Ahlawat, Seema,Gupta, Ranju
, p. 419 - 425 (2002)
A series of tricyclic nitrogen bridgehea...
Synthesis of [1,2-A]-fused tricyclic dihydroquinolines by palladiumcatalyzed intramolecular C-N cross-coupling of polarized heterocyclic enamines
Bro?, B?etislav,R??i?ková, Zdeňka,?im?nek, Petr
supporting information, p. 118 - 141 (2016/10/22)
A simple methodology for [1,2-A]-fused t...
Pyrrolopyrimidine Derivatives as Novel Inhibitors of Multidrug Resistance-Associated Protein 1 (MRP1, ABCC1)
Schmitt, Sven Marcel,Stefan, Katja,Wiese, Michael
, p. 3018 - 3033 (2016/05/19)
Five series of pyrrolo[3,2-d]pyrimidines...
Targeting the polyamine transport system with benzazepine- and azepine-polyamine conjugates
Tomasi, Sophie,Renault, Jacques,Martin, Bénédicte,Duhieu, Stephane,Cerec, Virginie,Le Roch, Myriam,Uriac, Philippe,Delcros, Jean-Guy
experimental part, p. 7647 - 7663 (2011/02/22)
The polyamine transport system (PTS) who...
SUBSTITUTED IMIDAZOHETEROCYCLE DERIVATIVES
-
Page/Page column 29, (2010/07/02)
The present invention provides substitut...
2525-16-8 Process route
-
-
105-60-2,9012-16-2
caprolactam
-
-
420-37-1
trimethoxonium tetrafluoroborate
-
-
2525-16-8
O-methylcaprolactim
| Conditions | Yield |
|---|---|
|
In
dichloromethane;
at 20 ℃;
|
94%
|
|
In
dichloromethane;
at 20 ℃;
for 18h;
|
|
|
In
dichloromethane;
|
|
|
|
|
|
|
|
|
caprolactam; trimethoxonium tetrafluoroborate;
In
dichloromethane;
at 23 ℃;
for 16h;
With
sodium hydrogencarbonate;
In
dichloromethane;
at 0 ℃;
for 0.5h;
|
|
|
In
dichloromethane;
|
-
-
105-60-2,9012-16-2
caprolactam
-
-
77-78-1
dimethyl sulfate
-
-
2525-16-8
O-methylcaprolactim
| Conditions | Yield |
|---|---|
|
at 75 ℃;
for 24h;
Sealed tube;
|
79%
|
|
In
benzene;
Heating;
|
40%
|
|
In
toluene;
for 16.75h;
Heating;
|
35%
|
|
With
sodium carbonate;
In
acetone;
for 20h;
Heating;
|
20%
|
|
In
benzene;
for 16h;
Heating;
|
|
|
at 80 - 90 ℃;
for 3h;
|
|
|
In
benzene;
for 3h;
Reflux;
|
2525-16-8 Upstream products
-
105-60-2
caprolactam
-
77-78-1
dimethyl sulfate
-
71-43-2
benzene
-
100-64-1
cyclohexanone-oxime
2525-16-8 Downstream products
-
2309-49-1
theacrine
-
116598-69-7
6,7,8,9-tetrahydro-5H-[1,2,4]triazolo[4,3-a]azepin-3-ylacetonitrile
-
100718-16-9
p -toluic acid-(4,5,6,7-tetrahydro-3H -azepin-2-yl ester)
-
109717-32-0
N -hexahydroazepin-2-ylidene-DL -phenylalanine
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